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# nanocrystalline metals prepared by high energy ball milling

### Fecht, H.J., Hellstern, E., Fu, Z. and Johnson, W.L. (1990 ...

Fecht, H.J., Hellstern, E., Fu, Z. and Johnson, W.L. (1990) Nanocrystalline Metals Prepared by High-Energy Ball Milling. Metallurgical and Materials Transactions A ...

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### Porous Nanocrystalline Alloys Prepared by High Energy Ball ...

Porous Nanocrystalline Alloys Prepared by High Energy Ball Milling p.1055 Microstructure Refinement of Cast Intermetallic Alloys - A New Application for Nano-Crystalline Powders

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### Nanocrystalline Diamond Particles Prepared by High-Energy ...

In this present work, nanodiamond (ND) particles were successfully prepared from commercial micron diamond powder at room temperature by high energy ball milling process using an oscillatory mill (SPEX8000). The size reduction and structural evolutions of the milled samples were investigated as a function of the milling time by means of X-ray diffraction, and field emission scanning electron ...

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### Atomic-scale structure of nanocrystalline ZrO prepared by ...

2005-6-23  Atomic-scale structure of nanocrystalline ZrO2 prepared by high-energy ball milling M. Gateshki and V. Petkov* Department of Physics, Central Michigan University, Mt. Pleasant, Michigan 48859, USA G. Williams Department of Biology, Central Michigan University, Mt. Pleasant, Michigan 48859, USA S. K. Pradhan

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### Amorphous and nanocrystalline Fe-Ti prepared by ball

nanocrystalline alloys2'3 in the hope that they may combine the advantages of the crystalline and amorphous phases with the disadvantages of neither. An alloy may be prepared in a nanocrystalline state by a variety of techniques, but probably the most attractive is high energy ball milling

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### The Structure of Nanocrystalline Iron and Tungsten Powders ...

The Structure of Nanocrystalline Iron and Tungsten Powders Prepared by High-Energy Ball Milling - Volume 35 Issue A Skip to main content Accessibility help We use cookies to distinguish you from other users and to provide you with a better experience on our websites.

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### Nanocrystalline metals prepared by low energy ball milling ...

1998-6-4  The influence of low energy ball milling on the crystallite size, lattice strain, and storage of deformation energies of elemental metal powders is studied. The formation of nanosized grains (5–25 nm) and enhancement of lattice strain up to 0.4% is found.

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### Nanocrystalline/nanoparticle ZnO synthesized by high ...

2012-11-1  Ball milling was performed in different milling times using a high energy planetary ball mill machine (Retsch PM100). The milling container was consisting of 15 balls with diameter of 20 mm confined in a 500 ml bowl. Both the ball and bowl materials were made from hardened chromium steels.

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### Fecht, H.J., Hellstern, E., Fu, Z. and Johnson, W.L. (1990 ...

Fecht, H.J., Hellstern, E., Fu, Z. and Johnson, W.L. (1990) Nanocrystalline Metals Prepared by High-Energy Ball Milling. Metallurgical and Materials Transactions A ...

More

### Porous Nanocrystalline Alloys Prepared by High Energy Ball ...

Porous Nanocrystalline Alloys Prepared by High Energy Ball Milling p.1055 Microstructure Refinement of Cast Intermetallic Alloys - A New Application for Nano-Crystalline Powders

More

### Nanocrystalline Diamond Particles Prepared by High-Energy ...

In this present work, nanodiamond (ND) particles were successfully prepared from commercial micron diamond powder at room temperature by high energy ball milling process using an oscillatory mill (SPEX8000). The size reduction and structural evolutions of the milled samples were investigated as a function of the milling time by means of X-ray diffraction, and field emission scanning electron ...

More

### Amorphous and nanocrystalline Fe-Ti prepared by ball

nanocrystalline alloys2'3 in the hope that they may combine the advantages of the crystalline and amorphous phases with the disadvantages of neither. An alloy may be prepared in a nanocrystalline state by a variety of techniques, but probably the most attractive is high energy ball milling

More

### Nanocrystalline ZnO Powder Prepared by High Energy Ball Mill

A nanocrystalline powder of nonstoichiometric vanadium carbide VC0.875 has been prepared by the high-energy ball milling method. The crystal structure, microstructure, morphology, and size ...

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### Hydrogenation of Nanocrystalline Mg2Ni Alloy Prepared by ...

Nanocrystalline Mg2Ni powders produced by high energy ball milling (HEBM) were subjected to further severe plastic deformation by cold rolling (CR) or equal-channel angular pressing (ECAP). The microstructure of the alloys have been analysed by the Convolutional whole profile fitting method of the X-ray line profiles. The hydrogenation behavior has been studied by absorption kinetic measurements.

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### Phonon density of states of nanocrystalline Fe prepared

2012-6-22  Phonon density of states of nanocrystalline Fe prepared by high-energy ball milling B. Fultz California Institute of Technology, mail 138-78, Pasadena, California 91125 J. L. Robertson Oak Ridge National Laboratory, P.O. Box 2008, Oak Ridge, Tennessee 37831 T. A. Stephens and L. J. Nagel

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### Nanocrystalline metals prepared by low energy ball milling ...

The influence of low energy ball milling on the crystallite size, lattice strain, and storage of deformation energies of elemental metal powders is studied. The formation of nanosized grains (5-25 nm) and enhancement of lattice strain up to 0.4% is found. Excess enthalpies of up to

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### Nanocrystalline metals and alloys prepared by mechanical ...

Pure metals with body-centered cubic (bcc) and hexagonal close-packed (hcp) structures are subjected to ball milling, resulting in a decrease of the average grain size to ≈9 nm for metals with ...

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### Atomic-scale structure of nanocrystalline \${\\mathrm{ZrO ...

2005-6-21  The atomic-scale structure of nanocrystalline ZrO 2 obtained by ball milling has been studied using high-energy x-ray diffraction and the atomic pair distribution function technique. The studies show that, upon relatively short milling times, the parent crystalline material, monoclinic ZrO 2, evolves into a nanocrystalline phase that is locally similar to monoclinic zirconia but shows a cubic ...

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### (PDF) Structural Investigations of Nanocrystalline Cu-Cr ...

PDF Cu-Cr-Mo alloy could be a suitable candidate material for collector electrodes in high-power microwave tube devices. An attempt has been made to... Find, read and cite all the research you ...

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### Synthesis and Piezoelectric Properties of Nanocrystalline ...

Synthesis and Piezoelectric Properties of Nanocrystalline PZT-Based Ceramics Prepared by High Energy Ball Milling Process January 2004 Journal of Materials Science 39(16):5431-5434

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### High energy ball milling process for nanomaterial synthesis

2021-3-8  For all nanocrystalline materials prepared by high-energy ball milling synthesis route, surface and interface contamination is a major concern. In particular, mechanical attributed contamination by the milling tools (Fe or WC) as well as ambient gas (trace impurities such as O 2 , N 2 in rare gases) can be problems for high-energy ball milling.

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### Preparation of nanocrystalline VO y by high-energy ball ...

2011-3-30  We report high-energy milling of macrocrystalline nonstoichiometric cubic vanadium monoxide (VO y) powder in a planetary ball mill lined with stabilized zirconia.The results indicate that milling of macrocrystalline VO y powder at 500 rpm for more than 2 h considerably broadens diffraction line profiles, with no changes in the crystal structure of the vanadium monoxide, VO 1.00.

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### Li Conductivity of Nanocrystalline Li4Ti5O12 Prepared by a ...

Li Conductivity of Nanocrystalline Li 4 Ti 5 O 12 Prepared by a Sol-Gel Method and High-Energy Ball Milling. Article Preview. Abstract: Spinel-type structured Li4+xTi5O12 (0 6 x 6 3 ) is actually one of the most promising anode materials for Li ion batteries. In its nanostructured form it is already used in some commercially available Li ion ...

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### Nanocrystalline metals prepared by low energy ball milling ...

The influence of low energy ball milling on the crystallite size, lattice strain, and storage of deformation energies of elemental metal powders is studied. The formation of nanosized grains (5-25 nm) and enhancement of lattice strain up to 0.4% is found. Excess enthalpies of up to

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### Mechanical behavior of bulk nanocrystalline copper alloys ...

2011-1-29  Copper alloys with different amounts of zinc were synthesized via high energy ball milling at liquid nitrogen and room temperature. Bulk samples were produced in situ by controlling the milling temperature. It is shown that temperature plays an important role in formation of artifact-free consolidated samples via its effect on defect formation and annihilation during the milling process.

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### An X-ray diffraction study of nanocrystalline titanium ...

A detailed X-ray line-broadening study in ball-milled Ti sample is presented. It is observed that ball milling leads to the formation of nanocrystalline grains and transform partially to an f.c.c. Ti-phase after 10 h of milling. Using a Rietveld analysis, the volume fraction of f.c.c. phase was found to be ∼24% with a crystallite size of ∼20 Å. The origin of high strains is probably the ...

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### Transformation of Goethite to Hematite Nanocrystallines by ...

2014-8-18  α -Fe 2 O 3 nanocrystallines were prepared by direct transformation via high energy ball milling treatment for α -FeOOH powder. X-ray diffraction, Rietveld analysis, TEM, and vibrating sample magnetometer (VSM) are used to characterize the samples obtained after several milling times. Phase identification using Rietveld analysis showed that the goethite is transformed to hematite ...

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### Anion diffusivity in highly conductive nanocrystalline ...

We report on the fluorine diffusivity in nanocrystalline BaF2 and CaF2 as well as in BaF2:CaF2 composites prepared by high-energy ball milling. Mechanical treatment of polycrystalline BaF2 together with CaF2 results in a nanocrystalline composite with an unexpectedly high

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### Structure and magnetic properties of nanocrystalline ...

2019-2-2  In this current study, nanocrystalline Dy powders were prepared by melt-spinning and subsequent high-energy ball-milling. The effect of ball-milling time on the structure and magnetic properties of the powders was studied. The crystal structure and ...

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### Aberystwyth University Li conductivity of nanocrystalline ...

2020-4-18  High-energy ball milling serves as a versatile tool to reduc e and control the particle size of ion con-ducting ceramics [1]. Depending on the milling conditions s et and the type of mill used to prepare the nanocrystalline samples, after a few hours of milling th e

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### Synthesis and characterization of CuInS2 nanocrystalline ...

2015-10-22  Nanocrystalline CuInS 2 particles have been synthesized from copper, indium, and sulfur powders by high-energy milling in a planetary mill in an argon atmosphere. Structural characterization of the prepared nanoparticles, including phase identification, Raman spectroscopy, specific surface area measurement, and particle size analysis were performed.

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### Metals Special Issue : High Energy Ball Milling and ...

2021-6-30  Dear Colleagues, High energy ball milling (HEBM) has attracted increasing attention within the various branches of the scientific community. The HEBM of powder mixtures in high-speed planetary ball mills, shakers and other milling equipment allows for the production of nanostructured composites (including reactive ones), solid solutions, metastable phases, pseudoalloys, and various other ...

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### Thermal analysis investigation of hydriding properties of ...

nanocrystalline Mg–Ni- and Mg–Fe-based alloys prepared by high-energy ball milling L.E.A. Berlouis,a) E. Cabrera, E. Hall-Barientos, and P.J. Hall Department of Pure and Applied Chemistry, University of Strathclyde, 295 Cathedral Street, Glasgow, G1 1XL, United Kingdom S.B. Dodd and S. Morris

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